Moura, Maria de Fátima Vitória deInácio, Maria Raquel Cavalcanti2014-12-172011-03-012014-12-172010-02-24INÁCIO, Maria Raquel Cavalcanti. Ferramentas quimiométricas aplicadas a classificação de amostras de leite em pó e quantificação de proteínas. 2010. 121 f. Dissertação (Mestrado em Físico-Química; Química) - Universidade Federal do Rio Grande do Norte, Natal, 2010.https://repositorio.ufrn.br/jspui/handle/123456789/17634In this work we used chemometric tools to classify and quantify the protein content in samples of milk powder. We applied the NIR diffuse reflectance spectroscopy combined with multivariate techniques. First, we carried out an exploratory method of samples by principal component analysis (PCA), then the classification of independent modeling of class analogy (SIMCA). Thus it became possible to classify the samples that were grouped by similarities in their composition. Finally, the techniques of partial least squares regression (PLS) and principal components regression (PCR) allowed the quantification of protein content in samples of milk powder, compared with the Kjeldahl reference method. A total of 53 samples of milk powder sold in the metropolitan areas of Natal, Salvador and Rio de Janeiro were acquired for analysis, in which after pre-treatment data, there were four models, which were employed for classification and quantification of samples. The methods employed after being assessed and validated showed good performance, good accuracy and reliability of the results, showing that the NIR technique can be a non invasive technique, since it produces no waste and saves time in analyzing the samplesapplication/pdfAcesso AbertoLeite em póInfravermelho próximoSIMCAPLSPCRMilk powderNear infraredSIMCAPLSPCRmasterThesisCNPQ::CIENCIAS EXATAS E DA TERRA::QUIMICA