Microstructural study of neodmium nickelate doped with strontium synthesized by gelatin method

dc.contributor.authorMartinelli, Antonio Eduardo
dc.contributor.authorOliveira, Rosane Maria Pessoa Betânio
dc.contributor.authorPimentel, Patrícia Mendonça
dc.contributor.authorAraújo, José Humberto de
dc.contributor.authorMelo, Dulce Maria de Araújo
dc.contributor.authorMelo, Marcus Antônio de Freitas
dc.date.accessioned2021-09-14T14:08:38Z
dc.date.available2021-09-14T14:08:38Z
dc.date.issued2013-04-16
dc.description.resumoIn this work nickelate nanoparticles were synthesized using a simple and fast new route, which makes use of gelatin as an organic precursor in order to evaluate the performance of the synthesis method to obtain materials and the influence of the strontium replacement on the structural parameters of the powders. Samples of Nd2−𝑥Sr𝑥NiO4 (x = 0 and 0.4) were calcined at 700 and 900∘C at a heating of 10∘C/min for 4 hours. X-ray powder diffraction patterns were obtained for all the samples, and the Rietveld Method was applied in order to determine the crystallite size using Scherrer’s equation, the lattice parameters, and phase concentration. The results obtained using these techniques confirmed that the main crystal structure consists of the distorted K2NiF4-type tetragonal I4/mmm. In addition, scanning electron microscopy images revealed the formation of nanosized particlespt_BR
dc.identifier.citationOLIVEIRA, R. M. P. B.; PIMENTEL, P. M.; ARAðJO, J. H.; MELO, D. M. A.; MELO, M. A. F.; MARTINELLI, A. E.. Microstructural Study of Neodmium Nickelate Doped with Strontium Synthesized by Gelatin Method. Advances In Materials Science and Engineering, [S.L.], v. 2013, p. 1-5, 2013. Disponível em: https://www.hindawi.com/journals/amse/2013/926540/. Acesso em: 04 fev. 2021. http://dx.doi.org/10.1155/2013/926540.pt_BR
dc.identifier.doi10.1155/2013/926540
dc.identifier.issn1687-8442
dc.identifier.urihttps://repositorio.ufrn.br/handle/123456789/33396
dc.languageenpt_BR
dc.publisherHindawipt_BR
dc.rightsAttribution 3.0 Brazil*
dc.rights.urihttp://creativecommons.org/licenses/by/3.0/br/*
dc.subjectNeodmium Nickelate Dopedpt_BR
dc.subjectStrontium Synthesizedpt_BR
dc.titleMicrostructural study of neodmium nickelate doped with strontium synthesized by gelatin methodpt_BR
dc.typearticlept_BR

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